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A-Review-of-the-LPPM-IPMI-Platinum-Sponge-Analysis-Round-Robin-AR25.pdf

上传人: 小溪 编号:1165284 2026-03-14 19页 489.13KB

1、PGM Sponge Accreditation Platinum and Palladium introduced March 2021 Rhodium introduced January 2023 The most commonly used form of PGMs LPPM Members requested an accreditation system To secure and improve technical and responsible sourcing standardsPGM Sponge Accreditation Accreditation applicatio

2、n process is very similar to the Good Delivery(GD)application process Proactive Monitoring(PAM)process is also very similar and is integrated with the current GD programme Additional tests for oxygen content and sponge homogeneity Sponge Accredited refiner lists published by the LPPMInterlaboratory

3、Round RobinHigh Grade Platinum Sponge 99.95%Samples produced and certified by Johnson Matthey UK Results collated and distributed confidentially by the IPMI LPPM Good Delivery RefinersIPMI Sampling&Analytical Committee30 laboratories reported results22 were Good Delivery Refiner accredited laborator

4、iesInterlaboratory Round RobinReporting InstructionsAssay for fineness,impuritiesLoss on Reduction/Ignition or oxygen contentReport methodology and rate experience(1 to 5)Results useful for ISO 17025 accreditationInterlaboratory Round RobinInterlaboratory Round RobinAnalyteMeanMedianCERT Value#of La

5、bs ReportingPt%99.98599.98799.98030Major ImpuritiesNa(ppm)66737420Os25264519Ni23211929K19203120Pd991227Fe74323Cr53323Au43320Mo3321599.97299.97599.97699.97799.97899.98099.98099.98199.98299.98299.98399.98499.98599.98699.98699.98699.98799.98799.98799.98799.98799.98899.98899.98999.99099.990 99.99099.993

6、99.99499.99599.99999.985399.964599.969599.974599.979599.984599.989599.994599.9995WTCJK7CERTV5QNIGFMZ14ALX3RO2PSYDHBIPMI-LPPM Platinum Round RobinPlatinum Purity%Mean=99.985%Median=99.987%ParticipantGroupAverage95%Confidence Interval1 x Sigma2 x SigmaAverage w.95%Confidence Interval,Replicates0.25.05

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1. **PGM海绵认证**:2021年3月引入铂、钯,2023年1月引入铑,旨在提升技术及负责任采购标准,申请流程与Good Delivery(GD)类似,新增氧含量和海绵均匀性测试。 2. **实验室间联合测试**:30家实验室参与高纯度铂海绵(~99.95%)测试,22家为GD认证实验室。铂纯度均值99.985%(中位数99.987%),主要杂质如钠(66ppm)、锇(25ppm)等。 3. **结果应用**:测试数据有助于ISO 17025认证,未来将组织铑海绵联合测试。
**PGM认证新标准?** **铂金纯度如何测?** **实验室能力哪家强?**
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